May 23 – 25, 2023
FTU, TLK and IAP
Europe/Berlin timezone

Setup and characterization of a confocal Raman imaging microscope built for the measurement of tritiated samples

May 24, 2023, 2:00 PM
1h 30m
R410 (B401)

R410

B401

Poster presentations Poster session

Speaker

Genrich Zeller (KIT-TLK)

Description

In recent years, there has been a growing interest in conducting in-situ Raman measurements on tritium-loaded graphene or graphene-like samples due to proposals in neutrino physics programs like KATRIN and PTOLEMY. A confocal Raman microscope (CRM), which can used for spatio-chemical analysis of these samples, could become radioactive contaminated due to post-loading desorption of tritiated species. Therefore, a suitable CRM has to (i) comply with tritium-safety regulations, (ii) should have a minimal number of parts exposed to contamination, and (iii) can allow for future integration into a tritium glovebox system.
In this work, the setup and the design of a self-built CRM are presented, as well as selected characterization and Raman imaging measurements. Additionally, the status of a graphene-loading chamber with in-situ resistivity and temperature measurements is shown.

Primary authors

Genrich Zeller (KIT-TLK) Deseada Diaz Barrero Dr Magnus Schlösser (Tritium Laboratory Karlsruhe - Institute of Astroparticle Physics) Simon Niemes (IAP-TLK) Mr Paul Wiesen (IAP-TLK) Beate Bornschein (Karlsruhe Institute of Technology, Institute for Astroparticle Physics) Helmut Telle (Universidad Autonoma de Madrid)

Presentation materials

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